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BU/EQ/Boldenone Undecylenate CAS注入のための13103-34-9無し

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BU/EQ/Boldenone Undecylenate CAS注入のための13103-34-9無し

BU / EQ / Boldenone Undecylenate CAS No 13103-34-9 For Injection
BU / EQ / Boldenone Undecylenate CAS No 13103-34-9 For Injection

大画像 :  BU/EQ/Boldenone Undecylenate CAS注入のための13103-34-9無し ベストプライス

商品の詳細:

起源の場所: 湖北
ブランド名: DKY
証明: COA
モデル番号: 13103-34-9

お支払配送条件:

最小注文数量: 10g
パッケージの詳細: 1kg/bottle
受渡し時間: 5-7の仕事日
支払条件: T/T、ウェスタン・ユニオン、MoneyGram
供給の能力: 1年ごとの800kg
詳細製品概要
Cas: 13103-34-9 分子方式: C30H44O3
分子量: 452.67 EINECS: 236-024-5
沸点: 760のmmHgの553.2±50.0 °C 密度: 1.05±0.1 g/cm3
フラッシュ: 232.215 ° C 蒸気圧: 25°Cの0mmHg
指定: 98% 出現: 薄黄色の粘性液体
ハイライト:

13103-34-9

,

Boldenone Undecylenate

BU/EQ/Boldenone undecylenateCAS no: 13103-34-9 yellow liquid for injection
 
Basic parameter:
Product name :Boldenoneundecylenate
Nickname: Parenabol; Vebonol; Androsta-1, 4-dien-3-one, 17-(1-oxo-10-undecenyl) foxy--(17. Beta.) -; BoldenoneUndeclyenate; 17beta-(1-Oxo-10-undecenyloxy) androsta-1, 4- dien - 3 - one; Estra - 4, 9 - diene - 3 in 2 - dione (boldenoneUndecylenate); BoldenoneUndecylenateInjection; Boldenoeundecylenate
CAS no. : 13103-34-9
Molecular formula: C30H44O3
Molecular weight: 452.67
EINECS no. : 236-024-5
Boiling point: 553.2±50.0 °C at 760 mmHg
Density: 1.05±0.1 g/cm3
Flash: 232.215 ° C
Vapor pressure: 0mmHg at 25°C
Specifications: 98%
Appearance: Light yellow viscous liquid
 
Certificate of Analysis:
Product: Boldenone Undecylenate
Batch No.: 20200503 Mfg. Date: 2020-05-19 Analysis Date: 2020-05-21
Quantity: 50.0KG CAS No: 13103-34-9 Exp. Date: 2022-05-18
Storage: Preserve in tight, light-resistant containers. Standard: IN-HOUSE
ITEM AND RESULT
Item Specification Result
Characters

From pale yellow to clear at room termp.

Odourless or with slight characteristic odour

Complies
Solubility Practically insoluble in water, soluble in ethanol, chloroform, acetone dioxan, vegetable oils Complies
Identification A. UV Complies
B. IR
C. TLC
Specific Rotation +28.0° ~ +35.0° +30.9°
Density 1.020~1.035 1.028
Loss on Drying ≤0.5% 0.31%
Free Undecylenate ≤0.45% 0.29%
Related Substances Total Impurities ≤3.0% 0.87%
Assay ≥97% (HPLC) 99.13%
Conclusion: Complies with the IN-HOUSE Standard
Operator   Review   Q.C. Manager  
 
Product series:
BU/EQ/Boldenone Undecylenate CAS注入のための13103-34-9無し 0
 
Application:
Baodanone undecenoate is a chemical intermediate. The intermediate L, 4-androstene-17SS-3-11enoate, could be prepared from testosterone undecenoate as starting material, and further reacted with glacial acetic acid, pentanol and mercury to produce baotanone undecenoate.
 
Step 1: The synthesis of L, 4- androstene-17SS-3-eleven enolates
In 200 ml of tert-butyl ether, 4.54 g of 44-androenone 17 -3-11enone [testosterone undecenone] was added. 6.0g mercury was added in a nitrogen atmosphere and stirred continuously. 3.70g of selenium dioxide was dissolved in the mixture. The cooled reaction solution was filtered to separate selenium, mercury selenide and mercury, diluted with ethyl acetate, and then shaken repeatedly with ammonium sulfide and sodium carbonate solutions, washed with water, dried and evaporated by sodium sulfate. The result is 4.1g of coarse L, 4-androstenediene-17/3-3-11-enonate, which is a thick brown oil. It was dissolved in hexane and adsorbed under the action of alumina. Eluent with hexane, hexane-benzene 1:1 and benzene was used to obtain 3.2GL, 4-androstene-17SS-3-11enoate.
 
Step 2: Synthesis of baodanone undecenoate
4.5g l, 4-androstene-17SS-3-11-enenate, amyl alcohol and 5.0ml glacial acetic acid were added to 200mL solution. 12.0g mercury was added to stir vigorously under nitrogen atmosphere. 7.4g selenium dioxide was dissolved in 330ml mixture at reflux-temperature and pentanol was added. The mixture is then stirred in a nitrogen atmosphere to reflux for another 20 hours. Cooling reaction solution, mercury selenide and mercury separation, diluted with ethyl acetate, thoroughly washed with ammonium sulfide and soda solution, dried and evaporated. The obtained crude product was dissolved in hexane and coated with alumina in hexane. It was eluted with hexane, hexane - benzene 1∶1 and benzene to obtain 2.7g baotanone undecenoate.

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